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Mechanisms and prevention of trifluoroacetylation in solid-phase peptide synthesis
A novel mechanism for trifluoroacetylation in solid-phase peptide synthesis, independent of the coupling step, has been elucidated. It involves the presence of trifluoroacetoxymethyl groups on the resin support, which react with resin-bound amines by an intersite nucleophilic reaction. The trifluoro...
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| Main Authors: | , , , |
|---|---|
| Format: | Artigo |
| Jezik: | en |
| Izdano: |
1979
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| Teme: | |
| Online dostop: | https://ncbi.nlm.nih.gov/pmc/articles/PMC383561/ https://ncbi.nlm.nih.gov/pubmed/287055 |
| Oznake: |
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